Multiresidue Analysis of Pesticides in Fruits and Vegetables Using UPLC-MS/MS

Library Number:
APNT134942539
Part Number:
720006039EN
Author(s):
Dimple Shah, Naren Meruva, and Gareth Cleland
Source:
Waters
Content Type:
Application Notes
Content Subtype:
Application Notes
Related Products:
 
 
 
 
 

In this application note, we describe the development of a multi-residue method for the routine determination of 190 pesticide residues in various fruit and vegetable matrices using UPLC-MS/MS. White grapes and green beans were selected for this application due to their relatively increased complexity, since they contain chlorophylls which are known to affect the extraction efficiency of pesticides from food matrices.

A generic QuEChERS sample extraction procedure was used to extract the pesticides from the fruit and vegetable samples, followed by rapid and high resolution UPLC separation and trace level detection of pesticides using the Xevo TQ-S micro.

Application benefits include:

  • Multi-residue method for 190 pesticides in fruit and vegetable commodities showing excellent recoveries and precision at or below EU MRL.
  • Detection of incurred residues confirmed in compliance with SANTE 11945/2015 guidelines.
  • Method readily extendable for additional pesticides of interest, using DisQuE variations, MS/MS method database, and easily updated reporting criteria.

View the Application Note



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